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2 article(s) from Kitson, Philip J

The digital code driven autonomous synthesis of ibuprofen automated in a 3D-printer-based robot

Philip J. Kitson,
Stefan Glatzel and
Leroy Cronin

Beilstein J. Org. Chem. 2016, 12, 2776–2783, doi:10.3762/bjoc.12.276

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Figure 1: Prusa i3 RepRap printer modified for the automated synthesis of ibuprofen. Left: Full view of robot...

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Scheme 1: Synthetic route chosen for automated synthesis robot.

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Figure 2: Top: The three reaction vessels printed for ibuprofen synthesis on different scales; bottom left: i...

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Scheme 2: The digitisation of the synthesis of ibuprofen. This flow diagram shows the individual steps of the...

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Full Research Paper

Published 19 Dec 2016

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3D-printed devices for continuous-flow organic chemistry

Vincenza Dragone,
Victor Sans,
Mali H. Rosnes,
Philip J. Kitson and
Leroy Cronin

Beilstein J. Org. Chem. 2013, 9, 951–959, doi:10.3762/bjoc.9.109

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Figure 1: Schematic representation of the 3D-printed reactionware devices employed in this work showing the i...

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Figure 2: Flow system setup, where a R1 is connected to the syringe pumps and the ATR-IR flow cell with stand...

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Figure 3: Carbonyl compounds and primary amines used in the syntheses reported in this work. Carbonyl compoun...

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Figure 4: ATR-IR spectra of the synthesis of compounds 3b (on the left) and 3d (on the right). The spectrum o...

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Figure 5: (a) IR spectra of benzaldehyde at different concentrations. The solvent peak at 1022 cm⁻¹ remains c...

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Figure 6: Comparison of the IR spectra of imine 3a, derived from benzaldehyde (1a) and aniline (2a), synthesi...

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Figure 7: Representation of the setup for the two-step flow reaction employed in this work. The first reactor...

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Figure 8: Example of an ATR-IR graph in which an imine spectrum is compared with the reduced imine spectrum.

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Full Research Paper

Published 16 May 2013

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